HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → 4-(Chloromethyl)benzophenone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | 4-Methylbenzophenone | HCID 8652 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Solvent | Chlorobenzene | HCID 7964 | — |
| Product | 4-(Chloromethyl)benzophenone | HCID 3016376 | — |
Reaction Steps
196.2 g of 4-methylbenzophenone are dissolved in chlorobenzene and then gassed at 80° C. in the presence of 1.6 g of AIBN (azodiisobutyronitrile) with a total of 71.0 g of chlorine. The reaction mixture is concentrated and the solid material obtained recrystallized from 1 L of ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05859084 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-e7340966d1a240309ff577fc36a68f15 |
| Source note | uspto-grants-1999_01 |