HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(N-formylaminomethyl)benzophenone → (4-(Aminomethyl)phenyl)(phenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(N-formylaminomethyl)benzophenone | HCID 53721082 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | (4-(Aminomethyl)phenyl)(phenyl)methanone | HCID 2760963 | — |
Reaction Steps
70 g of 4-(N-formylaminomethyl)benzophenone are stirred in a mixture of 40 g of concentrated hydrochloric acid and 100 g of ethanol for 5 hours at 50° C. The alcohol is then removed by distillation and the pH is adjusted to 10 with sodium hydroxide solution. 4-aminomethylbenzophenone precipitates as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05859084 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-8df23931cdc646c2a417537deeb17402 |
| Source note | uspto-grants-1999_01 |