HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15334721, compound → {4-[(Methylamino)methyl]phenyl}(phenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15334721 | HCID 15334721 | — |
| Reactant | Hydrate;hydrochloride | HCID 21885828 | — |
| Product | {4-[(Methylamino)methyl]phenyl}(phenyl)methanone | HCID 15334722 | 86.3% |
Reaction Steps
22 g of 4-(N-acetyl-N-methylaminomethyl)benzophenone are refluxed in 100 mL of 1:1 -HCl/water mixture (by volume) for 7 hours. From the reaction mixture there are isolated 16 g of 4-(N-methylaminomethyl)benzophenone. HNMR: δ=1.7 (1H, NH), 2.5 (3H, NCH3), 3.9 (2H, NCH2), 7.1-7.4 (9H, aromatics).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05859084 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-7ffce052dddc4dcba74dd5192f872af7 |
| Source note | uspto-grants-1999_01 |