Hydrochloric Acid → HCID 178483608, compound

HRID 34305Notes

Reaction equation

HRID 34305 reaction equation
C(OC([NH:8][CH2:9][CH2:10][CH2:11][O:12][P:13](=[C:15]([CH2:17][N+:18]([CH3:21])([CH3:20])[CH3:19])[OH:16])=[O:14])=O)(C)(C)C.[ClH:22]>C(Cl)(Cl)Cl>[ClH:22].[ClH:22].[NH2:8][CH2:9][CH2:10][CH2:11][O:12][P:13](=[C:15]([CH2:17][N+:18]([CH3:19])([CH3:21])[CH3:20])[OH:16])=[O:14]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 178453565HCID 178453565, compound

Product 1

HCID 178483608HCID 178483608, compoundYield 96%

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

To a solution of 0.200 g (0.586 mmol) of 48 in 2 ml of chloroform was added 1 ml of HCl-saturated ether. The solution was shaken at room temperature for 20 minutes then concentrated to afford 0.190 g (96%) of the title compound as a colorless glass.

Workup

  1. concentrationthen concentrated

Sources & evidence

ORD record
ord-71904a040fa64e6a84cc8d2d686eb0c7
Source dataset
uspto-grants-1988_08
Patent number
US04761404

Reaction notes

Loading…