Methanesulfonamide → HCID 67703360, compound

Participants

Reaction Conditions

Reaction Steps

A stirring mixture of 2.6 0 grams (0.0050 mole) of 2-[5-ethyl-2-[3-fluoro-4-(4-chloro-5-difluoromethoxy-1-methylpyrazol-3-yl)phenoxymethyl]phenoxy]propanoic acid chloride and 0.52 gram (0.0055 mole) of methylsulfonylamine is heated at about 120° C. for two hours. The reaction mixture is then cooled and dissolved in about 35 mL of methylene chloride. The solution is washed with water, dried with magnesium sulfate, and filtered. The filtrate is concentrated under reduced pressure, yielding the title compound.

Provenance & Evidence