HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 70059665, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 54281626 | HCID 54281626 | — |
| Product | HCID 70059665 | HCID 70059665 | — |
Reaction Steps
A stirred mixture of 1-[4-(2,4-dibromo-benzoyl)-piperidin-1-yl]-ethanone (11.00 g, 28.3 mmol) and aqueous 5M hydrochloric acid (60 ml) was heated under reflux under nitrogen for 7 h. The mixture was evaporated in vacuo to give the title compound as a white solid (10.8 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05861414 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-684918e6067b4a388be21aac1e94ab7d |
| Source note | uspto-grants-1999_01 |