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HRID343898

反应详情

EQUATION

反应方程式

HRID 343898 的结构方程式

REACTANTS

反应物

2
结构：CN1CCC(c2c[nH]c3ccc(CC4NC(=O)NC4=O)cc23)CC1
HCID15233277

未命名化合物

结构：O.[Ba+2].[OH-].[OH-]
HCID17749100

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCC(c2c[nH]c3ccc(C[C@H](N)C(=O)O)cc23)CC1
HCID22852202

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A solution of the product from step (d) (2.4 g) and barium hydroxide hydrate (8.4 g) in water (50 ml) was refluxed for 72 hours, then cooled and evaporated in vacuo. The residue was taken up in hot methanol and filtered to remove barium salts.

WORKUP

后处理

  1. temperaturecooled
  2. customevaporated in vacuo
  3. filtrationfiltered
  4. customto remove barium salts