Hydrochloric Acid → HCID 52983856, compound

Participants

Reaction Steps

413 g of the proline benzylamide obtained in this way were dissolved in 400 ml of isopropanol. 630 ml of a saturated solution of HCl in isopropanol were added, the resulting suspension was stirred at 0°-5° C. for 2 h, and the solid was filtered off with suction and washed twice with 250 ml of isopropanol. The residue was dried at 50° C. under reduced pressure to obtain 401 g of proline benzylamide hydrochloride; aD20 :--45°

Provenance & Evidence