HuagongsheHuagongshe Chemistry Print Report · For research reference only
[(4-Chlorobutane-1-sulfonyl)methyl]benzene → HCID 70076541, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | [(4-Chlorobutane-1-sulfonyl)methyl]benzene | HCID 284426 | — |
| Reactant | 4-amino-5-chloro-2-methoxy-N-(piperidin-4-ylmethyl)benzamide dihydrochloride | HCID 69966330 | — |
| Product | HCID 70076541 | HCID 70076541 | 65.4% |
Reaction Steps
4-Amino-5-chloro-2-methoxy-N-(piperidin-4-ylmethyl)benzamide dihydrochloride (2 g) and 4-(benzylsulfonyl)butyl chloride (1.46 g) were reacted and treated in the same manner as in Example 199 to give 0.96 g of 4-amino-N-((1-(4-(benzylsulfonyl)butyl)piperidin-4-yl)-methyl)-5-chloro-2-methoxybenzamide hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05864039 |
| Source dataset | uspto-grants-1999_01 |
| ORD ID | ord-ed16b25ad5bb435ba8bc084aae3d0640 |
| Source note | uspto-grants-1999_01 |