HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic acid--N-(pyridin-4-yl)acetamide (1/1) → HCID 70155070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic acid--N-(pyridin-4-yl)acetamide (1/1) | HCID 67923113 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Adams' catalyst | HCID 345198 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 70155070 | HCID 70155070 | — |
Reaction Steps
A solution of the product of Example 2 (75 g) in 750 mL acetic acid was reduced over PtO2 catalyst at 60 psi hydrogen atmosphere at 60° C. for 7 hours. The solution was filtered, concentrated and triturated with ether to afford the title compound quantitatively as a white solid which was used directly in subsequent reactions.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05053413 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-76012d890f2b4e97bf59c6f39a205ece |
| Source note | uspto-grants-1991_10 |