HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dibromoethane → HCID 13061935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dibromoethane | HCID 7839 | — |
| Reactant | 1-Bromo-2-Chloroethane | HCID 7849 | — |
| Reactant | diethyl 1H-pyrazole-3,5-dicarboxylate | HCID 142184 | — |
| Reactant | HCID 13061935 | HCID 13061935 | — |
| Product | HCID 13061935 | HCID 13061935 | — |
| Product | HCID 86745115 | HCID 86745115 | — |
Reaction Steps
When an equivalent amount of 1-methyl-5-(2-chloroethylthio)-1H-tetrazole is substituted for 3,5-diethoxycarbonyl-1H-pyrazole and an equivalent amount of 2-bromochloroethane is substituted for 1,2-dibromoethane in the procedure of Example 4, 2-(1-methyl-5-(2-chloroethylthio)-1H-tetrazol-5-yl)ethyl chloride is isolated after column chromatography 1-methyl-5-(2-chloroethylthio)-1H-tetrazole, Aldrich, 59%, A).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05053411 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-33c63c1151b64ab8bcd70285ad388f45 |
| Source note | uspto-grants-1991_10 |