HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 67925092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 13812588 | HCID 13812588 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67925092 | HCID 67925092 | 83.5% |
Reaction Steps
10.8 g of 3-(4-methyloxazol-2-yl)-pyridine and 19.4 g of methyl iodide are mixed together in 140 cm3 of ethanol, then heated under reflux for 6 hours. The solvent is evaporated, the residue is crystallized from a mixture of ethanol and ether and 17 g of expected product is obtained, which is recrystallized from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05053416 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-a39e6049d82d47178f3e6a2f5588b23f |
| Source note | uspto-grants-1991_10 |