Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Methyl N-acetyl-beta-alaninate | HCID 12859671 | — |
| Product | 138148-37-5 | HCID 19805630 | 62.6% |
Reaction Steps
A mixture of 0.42 g of ethanolamine and 1.0 g of N-acetyl-β-alanine methyl ester was heated at 85° C. for 4 hours. The resulting yellow oil solidified upon cooling and was crystallized from acetonitrile, giving 0.75 g of the desired compound as a white solid, mp 122-125° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05053426 |
|---|
| Source dataset | uspto-grants-1991_10 |
|---|
| ORD ID | ord-d65c514e95c846b281f498b931691aab |
|---|
| Source note | uspto-grants-1991_10 |
|---|
