Diethyl Ether → HCID 86745121, compound

Participants

Reaction Steps

A 0.5 g portion of N-(4-hydroxy-12(Z)-eicosenyl)-acetamide was stirred with 0.44 g of pyridinium chlorochromate in 15 ml of dichloromethane for 2 hours. This mixture was poured into 50 ml of ether and filtered through hydrous magnesium silicate. The filtrate was evaporated giving 0.24 g of the desired product as a pale yellow solid, mp 51-52° C.

Provenance & Evidence