HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanedithiol → HCID 15020331, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanedithiol | HCID 8013 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 86745117 | HCID 86745117 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15020331 | HCID 15020331 | 95.9% |
Reaction Steps
A solution of trans-5-cyano-1,1-dimethyl-3-azido-indan-2-ol (0.93g), triethylamine (1.2 ml) and 1,3-propanedithiol (0.9 ml) in dry methanol (20 ml) was stirred at room temperature for 48h. After filtration, the solution was evaporated in vacuo to give the title compound (0.79g) as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05053427 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-9337b30c5a31462b9be6b7f46ca11645 |
| Source note | uspto-grants-1991_10 |