HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → 2-(4-Hexyl-phenyl)-5-(4-propyl-benzyloxy)-pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-(4-Hexylphenyl)-5-hydroxypyrimidine | HCID 604041 | — |
| Reactant | 1-(Bromomethyl)-4-propylbenzene | HCID 22246866 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 2-(4-Hexyl-phenyl)-5-(4-propyl-benzyloxy)-pyrimidine | HCID 19992771 | — |
Reaction Steps
A mixture of 10.2 g of 5-hydroxy-2-(4-n-hexyl-phenyl)-pyrimidine, 8.6 g of 4-n-propylbenzyl bromide, 8.6 g of potassium carbonate and 50 ml of dimethylformamide are warmed at 90° for 10 hours. Conventional work-up gives 2-(4-n-hexylphenyl)-pyrimidin-5-yl p-n-propylbenzyl ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05055221 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-9931acab2c63485a8ba2b4a7b0f26312 |
| Source note | uspto-grants-1991_10 |