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HRID344978

反应详情

EQUATION

反应方程式

HRID 344978 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCCCCCc1ccc(-c2ncc(O)cn2)cc1
HCID604041

2-(4-Hexylphenyl)-5-hydroxypyrimidine

C16H20N2O

结构：CCCc1ccc(CBr)cc1
HCID22246866

1-(Bromomethyl)-4-propylbenzene

C10H13Br

PRODUCTS

生成物

1
结构：CCCCCCc1ccc(-c2ncc(OCc3ccc(CCC)cc3)cn2)cc1
HCID19992771

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

A mixture of 10.2 g of 5-hydroxy-2-(4-n-hexyl-phenyl)-pyrimidine, 8.6 g of 4-n-propylbenzyl bromide, 8.6 g of potassium carbonate and 50 ml of dimethylformamide are warmed at 90° for 10 hours. Conventional work-up gives 2-(4-n-hexylphenyl)-pyrimidin-5-yl p-n-propylbenzyl ether.

WORKUP

后处理

  1. temperatureare warmed at 90° for 10 hours