HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 178444428, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | 4-(2-(4-Pentoxyphenyl)-ethynyl)-phenyl-sulfur pentafluoride | HCID 86745128 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | HCID 178444428 | HCID 178444428 | — |
Reaction Steps
A mixture of 11.4 g of 4-(2-(4-trans-pentylcyclo-hexyl)-ethynyl)-phenyl sulfur pentafluoride (prepared as in EXAMPLE 7), 50 ml of toLuene and 10 mg of palladium-on-active charcoal is hydrogenated at room temperature under normal pressure. The solid constituents are filtered off and the filtrate is concentrated and worked up in the customary manner to give 4-(2-(trans-4-pentyl-cyclohexyl)-ethyl)-phenyl-sulfur pentafluoride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05055223 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-1ca769012fb6453a8f69932cfa19f8f2 |
| Source note | uspto-grants-1991_10 |