Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 344984Generated: October 26, 2026

Toluene → HCID 178444428, compound

https://huagongshe.com/reaction/344984

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTolueneHCID 1140—
Reactant4-(2-(4-Pentoxyphenyl)-ethynyl)-phenyl-sulfur pentafluorideHCID 86745128—
CatalystPalladiumHCID 23938—
ProductHCID 178444428HCID 178444428—

Reaction Steps

A mixture of 11.4 g of 4-(2-(4-trans-pentylcyclo-hexyl)-ethynyl)-phenyl sulfur pentafluoride (prepared as in EXAMPLE 7), 50 ml of toLuene and 10 mg of palladium-on-active charcoal is hydrogenated at room temperature under normal pressure. The solid constituents are filtered off and the filtrate is concentrated and worked up in the customary manner to give 4-(2-(trans-4-pentyl-cyclohexyl)-ethyl)-phenyl-sulfur pentafluoride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05055223
Source datasetuspto-grants-1991_10
ORD IDord-1ca769012fb6453a8f69932cfa19f8f2
Source noteuspto-grants-1991_10