Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Allyl chloride | HCID 7850 | — |
| Reactant | Anthracene | HCID 8418 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 285302 | HCID 285302 | — |
Reaction Steps
Anthracene (75 gm) was combined with allyl chloride (150 gm) and benzene (375 gm) in a Parr bomb and heated to 220° C. for 13 hours. The contents were filtered and the benzene was removed on a rotary evaporator. The residue was recrystallized from ethanol to provide the product as a white solid (mp=108-111° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05055468 |
|---|
| Source dataset | uspto-grants-1991_10 |
|---|
| ORD ID | ord-0904ad31196348e2ad049f49ce6088bc |
|---|
| Source note | uspto-grants-1991_10 |
|---|
