Allyl chloride → HCID 285302, compound

HRID 345015Notes

Reaction equation

HRID 345015 reaction equation
[CH:1]1[C:14]2[C:5](=[CH:6][C:7]3[C:12]([CH:13]=2)=[CH:11][CH:10]=[CH:9][CH:8]=3)[CH:4]=[CH:3][CH:2]=1.[CH2:15]([Cl:18])[CH:16]=[CH2:17]>C1C=CC=CC=1>[Cl:18][CH2:15][CH:16]1[CH:6]2[C:7]3[CH:8]=[CH:9][CH:10]=[CH:11][C:12]=3[CH:13]([C:14]3[C:5]2=[CH:4][CH:3]=[CH:2][CH:1]=3)[CH2:17]1

Participants

4

Reactant 2

HCID 7850Allyl chlorideHCID 8418Anthracene

Product 1

HCID 285302HCID 285302, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Conditions

Temperature
220 °C

Procedure

Anthracene (75 gm) was combined with allyl chloride (150 gm) and benzene (375 gm) in a Parr bomb and heated to 220° C. for 13 hours. The contents were filtered and the benzene was removed on a rotary evaporator. The residue was recrystallized from ethanol to provide the product as a white solid (mp=108-111° C.).

Workup

  1. filtrationThe contents were filtered
  2. customthe benzene was removed on a rotary evaporator
  3. customThe residue was recrystallized from ethanol

Sources & evidence

ORD record
ord-0904ad31196348e2ad049f49ce6088bc
Source dataset
uspto-grants-1991_10
Patent number
US05055468

Reaction notes

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