反应详情

温度

220 °C

Anthracene (75 gm) was combined with allyl chloride (150 gm) and benzene (375 gm) in a Parr bomb and heated to 220° C. for 13 hours. The contents were filtered and the benzene was removed on a rotary evaporator. The residue was recrystallized from ethanol to provide the product as a white solid (mp=108-111° C.).

1. filtrationThe contents were filtered
2. customthe benzene was removed on a rotary evaporator
3. customThe residue was recrystallized from ethanol