HRID345017

反应详情

EQUATION

反应方程式

HRID 345017 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
210 °C

PROCEDURE

实验过程

Anthracene (45.4 gm) was combined with allyl alcohol (90.8 gm) and benzene (260 ml) in a Parr bomb and heated to 210° C. for 12 hours. The benzene was removed on a rotary evaporator and the residue was recrystallized from n-heptane to provide the product as a white solid (mp=104-105° C.).

WORKUP

后处理

  1. customThe benzene was removed on a rotary evaporator
  2. customthe residue was recrystallized from n-heptane