참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Allyl Alcohol | HCID 7858 | — |
| 반응물 | Anthracene | HCID 8418 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 9,10-Dihydro-9,10-ethanoanthracene-11-methanol | HCID 244379 | — |
반응 단계
Anthracene (45.4 gm) was combined with allyl alcohol (90.8 gm) and benzene (260 ml) in a Parr bomb and heated to 210° C. for 12 hours. The benzene was removed on a rotary evaporator and the residue was recrystallized from n-heptane to provide the product as a white solid (mp=104-105° C.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US05055468 |
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| 출처 데이터셋 | uspto-grants-1991_10 |
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| ORD ID | ord-26e8b67da6d0439bab031a0b94d37ce5 |
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| 출처 메모 | uspto-grants-1991_10 |
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