Formic Acid → N,N-bis-(3-chloroallyl) formamide

HRID 34508Notes

Reaction equation

HRID 34508 reaction equation
[Cl:1][CH:2]=[CH:3][CH2:4][NH:5][CH2:6][CH:7]=[CH:8][Cl:9].[CH:10](O)=[O:11]>>[Cl:1][CH:2]=[CH:3][CH2:4][N:5]([CH2:6][CH:7]=[CH:8][Cl:9])[CH:10]=[O:11]

Participants

3

Reactant 2

HCID 284Formic AcidHCID 53981628Bis-(3-chloroallyl)amine

Product 1

HCID 54053404N,N-bis-(3-chloroallyl) formamide

Procedure

Bis-(3-chloroallyl)amine (2.5 g, 0.015 mol) and 25 ml formic acid were combined and refluxed for 5 hours. The mixture was stripped under a vacuum from a hot-water bath. The yield was 2.6 g of the above-named product.

Workup

  1. temperaturerefluxed for 5 hours

Sources & evidence

ORD record
ord-bcd204024f554b92808722ea6d81a185
Source dataset
uspto-grants-1988_08
Patent number
US04762548

Reaction notes

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