HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formic Acid → N,N-bis-(3-chloroallyl) formamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formic Acid | HCID 284 | — |
| Reactant | Bis-(3-chloroallyl)amine | HCID 53981628 | — |
| Product | N,N-bis-(3-chloroallyl) formamide | HCID 54053404 | — |
Reaction Steps
Bis-(3-chloroallyl)amine (2.5 g, 0.015 mol) and 25 ml formic acid were combined and refluxed for 5 hours. The mixture was stripped under a vacuum from a hot-water bath. The yield was 2.6 g of the above-named product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04762548 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-bcd204024f554b92808722ea6d81a185 |
| Source note | uspto-grants-1988_08 |