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HRID345104

反应详情

EQUATION

反应方程式

HRID 345104 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)Oc1ccc([N+](=O)[O-])cc1
HCID82129

Carbonochloridic acid, 4-nitrophenyl ester

C7H4ClNO4

结构：OCCc1ccsc1
HCID83731

Thiophene-3-ethanol

C6H8OS

PRODUCTS

生成物

1
结构：O=C(OCCc1ccsc1)Oc1ccc([N+](=O)[O-])cc1
HCID57094331

未命名化合物

PROCEDURE

实验过程

Using the method of Example 7a, 3-thiopheneethanol was treated with 4-nitrophenyl chloroformate to afford, after purification by flash chromatography (EtOAc:hexane (1:9)), the title product (56%); TLC, Rf= 0.25, EtOAc:hexane (1:9).

WORKUP

后处理

  1. customto afford
  2. customafter purification by flash chromatography (EtOAc:hexane (1:9))