HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 178443208, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Phosphinic Acid | HCID 4124402 | — |
| Reactant | 6-Methyl-3-[1-(4-nitrophenoxy)tridecyl]-7H-1,2,4-triazolo[3,4-b][1,3,4]thiadiazine | HCID 15002716 | — |
| Product | HCID 178443208 | HCID 178443208 | — |
Reaction Steps
Process of claim 2 wherein 6-methyl-3-(1-[4-nitrophenoxy]tridecyl)-7H-1,2,4-triazolo[3,4-b]-[1,3,4]thiadiazine] is reacted with acetic anhydride, and the acylated intermediate thereby produced is reacted with HCl in the presence of hypophosphorous acid to produce 6-methyl-3-[1-(4-nitrophenoxy)tridecyl]-1H-pyrazolo-[5,1-c]-1,2,4-triazole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05055586 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-76ea142cde204b11a2af4ba7ec313a7d |
| Source note | uspto-grants-1991_10 |