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HRID345184

反应详情

EQUATION

反应方程式

HRID 345184 的结构方程式

REACTANTS

反应物

4
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(=O)OC(C)=O
HCID7918

Acetic anhydride

C4H6O3

结构：O=[PH2]O
HCID4124402

Phosphinic acid

H3O2P

结构：CCCCCCCCCCCCC(Oc1ccc([N+](=O)[O-])cc1)c1nnc2n1N=C(C)CS2
HCID15002716

6-Methyl-3-[1-(4-nitrophenoxy)tridecyl]-7H-1,2,4-triazolo[3,4-b][1,3,4]thiadiazine

C24H35N5O3S

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCC(Oc1ccc([N+](=O)[O-])cc1)c1n[nH]c2cc(C)nn12
HCID178443208

未命名化合物

PROCEDURE

实验过程

Process of claim 2 wherein 6-methyl-3-(1-[4-nitrophenoxy]tridecyl)-7H-1,2,4-triazolo[3,4-b]-[1,3,4]thiadiazine] is reacted with acetic anhydride, and the acylated intermediate thereby produced is reacted with HCl in the presence of hypophosphorous acid to produce 6-methyl-3-[1-(4-nitrophenoxy)tridecyl]-1H-pyrazolo-[5,1-c]-1,2,4-triazole.

WORKUP

后处理

  1. customthe acylated intermediate thereby produced