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HRID345194

反应详情

EQUATION

反应方程式

HRID 345194 的结构方程式

REACTANTS

反应物

2
结构：CCOS(=O)(=O)c1ccc(C)cc1
HCID6638

Benzenesulfonic acid, 4-methyl-, ethyl ester

C9H12O3S

结构：Cc1nc2ccccc2s1
HCID8446

2-Methylbenzothiazole

C8H7NS

PRODUCTS

生成物

1
结构：CC[n+]1c(C)sc2ccccc21.Cc1ccc(S(=O)(=O)O)cc1
HCID86745138

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)=O
溶剂HCID180

Acetone

C3H6O

CONDITIONS

反应条件

温度
150 °C

PROCEDURE

实验过程

2-Methylbenzothiazole (300 pbw) and ethyl p-toluenesulfonate (440 pbw) are heated with stirring to 150° C., the temperature rising to about 200° C. due to the exothermic reaction. After 10 minutes, the mixture is poured into 2000 pbw of acetone, and the product that precipitates is removed by filtration with suction, washed with acetone and dried over phosphorous pentoxide.

WORKUP

后处理

  1. customthe temperature rising to about 200° C. due to the exothermic reaction
  2. customthe product that precipitates
  3. customis removed by filtration with suction
  4. washwashed with acetone
  5. dry with materialdried over phosphorous pentoxide