HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl p-toluenesulfonate → HCID 86745141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl p-toluenesulfonate | HCID 6645 | — |
| Reactant | 2-Methylquinoline | HCID 7060 | — |
| Product | HCID 86745141 | HCID 86745141 | — |
Reaction Steps
2-Methyl-quinoline (71.5 pbw) and methyl-p-toluenesulfonate (102.3 pbw) are heated for about 10 minutes at 100° C. An exothermic reaction sets in, in which the mixture is heated to 180.C. After another 10 minutes the mixture is poured onto acetone, filtered with suction, washed with acetone and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05055579 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-d610caabd6674847a09a87c6df6e813e |
| Source note | uspto-grants-1991_10 |