HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14850786, compound → HCID 86743735, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14850786 | HCID 14850786 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86743735 | HCID 86743735 | — |
Reaction Steps
A solution of 1.0 g of cis-1-benzyloxycarbonyl-4-dimethylphosphonomethyl-2-piperidinecarboxylic acid in 30 ml of ethanol is hydrogenated at 3 atmospheres pressure over 500 mg of 10% palladium on carbon catalyst in 30 ml of ethanol. Filtration and removal of solvent affords cis-4-dimethylphosphonomethyl-2-piperidine-carboxylic acid as an amorphous solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05057506 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-611350e18b714c378860e1fe5ee2653f |
| Source note | uspto-grants-1991_10 |