HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylcyclohexyl 2-amino-alpha-methylbenzothiazole-6-acetate → 1-Adamantyl 2-amino-alpha-methylbenzothiazole-6-acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylcyclohexyl 2-amino-alpha-methylbenzothiazole-6-acetate | HCID 13754072 | — |
| Reactant | 1-Adamantyl 2-(p-aminophenyl)propionate | HCID 21298173 | — |
| Product | 1-Adamantyl 2-amino-alpha-methylbenzothiazole-6-acetate | HCID 54168576 | 83% |
Reaction Steps
Using the methpod similar to that used in the preparation of 1-methylcyclohexyl 2-amino-α-methylbenzothiazole-6-acetate, 19.1 g of 1-adamantyl 2-(p-aminophenyl)propionate were reacted to obtain 18.97 g (83% yield) of 1-adamantyl 2-amino-α-methylbenzothiazole-6-acetate as a creamy white solid melting at 151°-153° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04762840 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-fcd899a0ea594fffac41dad66a1efbd7 |
| Source note | uspto-grants-1988_08 |