HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-chloro-9-methyl-9H-purine → 6-Chloro-2,9-dimethyl-9H-purine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-chloro-9-methyl-9H-purine | HCID 94844 | — |
| Reactant | 5-Amino-4-chloro-2-methyl-6-methylaminopyrimidine | HCID 15016714 | — |
| Product | 6-Chloro-2,9-dimethyl-9H-purine | HCID 15016715 | 97% |
Reaction Steps
This was prepared in a manner similar to that described in Example 9 for 6-chloro-9-methylpurine, except that 5-amino-4-chloro-2-methyl-6-methylaminopyrimidine was used as the starting material and the reaction was carried out at 60° C. for 6 hrs. The title compound was obtained in 97% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05057517 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-eb2e80a7f8994455ba4a6199d6b59f34 |
| Source note | uspto-grants-1991_10 |