HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 19992430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 19992424 | HCID 19992424 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 19992430 | HCID 19992430 | 69.1% |
Reaction Steps
Treatment of 4-[(4-aminophenoxy)methyl]-1-[4-pyridyl]piperidine (see Preparation 4) (0.567 g) with methanesulphonyl chloride (0.263 g) in pyridine (18 ml) according to the method of Example 1 gave the title compound, (0.50 g), m.p. 214°-215° (from ethanol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05057528 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-e1483b997f774af58453144e1bccc944 |
| Source note | uspto-grants-1991_10 |