Hydrochloric Acid → N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-ethylenediamine hydrochloride

HRID 34562Notes

Reaction equation

HRID 34562 reaction equation
[ClH:1].[CH3:2][C:3]([CH2:11][CH2:12][CH:13]=[C:14]([CH3:26])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:25])[CH2:19][CH2:20][CH:21]=[C:22]([CH3:24])[CH3:23])=[CH:4][C:5]([NH:7][CH2:8][CH2:9][NH2:10])=[O:6]>CO>[ClH:1].[CH3:2][C:3]([CH2:11][CH2:12][CH:13]=[C:14]([CH3:26])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:25])[CH2:19][CH2:20][CH:21]=[C:22]([CH3:24])[CH3:23])=[CH:4][C:5]([NH:7][CH2:8][CH2:9][NH2:10])=[O:6]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 53736300HCID 53736300, compound

Product 1

HCID 73762859N-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoyl)-ethylenediamine hydrochloride

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrogen chloride gas was passed through a methanol solution of N-(3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoyl)-ethylenediamine obtained in Example 9. The solvent was distilled off to afford 6.1 g of the title compound as a brown oil.

Workup

  1. distillationThe solvent was distilled off

Sources & evidence

ORD record
ord-e5287a1269dc4af9ad109a272fd9ba31
Source dataset
uspto-grants-1988_08
Patent number
US04762829

Reaction notes

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