HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 18780265, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | 1-(3-Bromopropyl)indole | HCID 11859027 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18780265 | HCID 18780265 | — |
Reaction Steps
3 g of 1-(3-bromopropyl)indole were treated with a 33% solution of methylamine in ethanol. The resulting solution was stirred for 6 hours. The solvent was evaporated and the residue was dissolved in 50 ml of dichloromethane and washed with a saturated sodium bicarbonate solution. The organic phase was dried and evaporated to give 2.30 g of 1-(3-methylaminopropyl)indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05057614 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-49fcbaa3aa6d44e88b0abf230c6c41ed |
| Source note | uspto-grants-1991_10 |