HRID345692
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
3 g of 1-(3-bromopropyl)indole were treated with a 33% solution of methylamine in ethanol. The resulting solution was stirred for 6 hours. The solvent was evaporated and the residue was dissolved in 50 ml of dichloromethane and washed with a saturated sodium bicarbonate solution. The organic phase was dried and evaporated to give 2.30 g of 1-(3-methylaminopropyl)indole.
WORKUP
后处理
- customThe solvent was evaporated
- dissolutionthe residue was dissolved in 50 ml of dichloromethane
- washwashed with a saturated sodium bicarbonate solution
- customThe organic phase was dried
- customevaporated