HRID345692

反应详情

EQUATION

反应方程式

HRID 345692 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

3 g of 1-(3-bromopropyl)indole were treated with a 33% solution of methylamine in ethanol. The resulting solution was stirred for 6 hours. The solvent was evaporated and the residue was dissolved in 50 ml of dichloromethane and washed with a saturated sodium bicarbonate solution. The organic phase was dried and evaporated to give 2.30 g of 1-(3-methylaminopropyl)indole.

WORKUP

后处理

  1. customThe solvent was evaporated
  2. dissolutionthe residue was dissolved in 50 ml of dichloromethane
  3. washwashed with a saturated sodium bicarbonate solution
  4. customThe organic phase was dried
  5. customevaporated