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Methanol → N-dodecylproline ethyl ester
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methanol | HCID 887 | — |
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | Dodecylamine | HCID 13583 | — |
| 反応物 | Ethyl 2,5-dibromopentanoate | HCID 11022534 | — |
| 溶媒 | Ethanol | HCID 702 | — |
| 生成物 | N-dodecylproline ethyl ester | HCID 54196315 | — |
反応手順
In 150 ml of ethanol was dissolved 22.8 g of ethyl 2,5-dibromovalerate, and 15 g of potassium carbonate was suspended in the solution. To the suspension was added dropwise a methanolic solution of 18.5 g of laurylamine under ice-cooling. After the addition, the reaction mixture was allowed by react at a refluxing temperature of methanol for 5 hours to obtain N-dodecylproline ethyl ester.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05059628 |
| 出典データセット | uspto-grants-1991_10 |
| ORD ID | ord-133022ee30e24a839e4911617c6226af |
| 出典メモ | uspto-grants-1991_10 |