HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tridecanoic acid → Tridecanoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tridecanoic acid | HCID 12530 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Tridecanoyl chloride | HCID 87288 | — |
Reaction Steps
To a benzene solution containing 5.0 g (0.023 mol) of tridecanoic acid was added 25 g of thionyl chloride, followed by refluxing for 5 hours. The excess of thionyl chloride and benzene were removed by distillation to obtain tridecanoyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05059628 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-b6fd7f8ab8d244baa08dccc98c1036ee |
| Source note | uspto-grants-1991_10 |