HRID345873

反应详情

EQUATION

反应方程式

HRID 345873 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a benzene solution containing 5.0 g (0.023 mol) of tridecanoic acid was added 25 g of thionyl chloride, followed by refluxing for 5 hours. The excess of thionyl chloride and benzene were removed by distillation to obtain tridecanoyl chloride.

WORKUP

后处理

  1. temperatureby refluxing for 5 hours
  2. customThe excess of thionyl chloride and benzene were removed by distillation