HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Methacrylate → HCID 19809267, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Methacrylate | HCID 6658 | — |
| Reactant | Maleimide | HCID 10935 | — |
| Catalyst | Azobisisobutyronitrile | HCID 6547 | — |
| Catalyst | 1-Dodecanethiol | HCID 8195 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19809267 | HCID 19809267 | 55.3% |
Reaction Steps
In a manner identical to Example 4, 10 g of maleimide, 10 g of methyl methacrylate, 0.8 g of AIBN, and 0.1 g of dodecanethiol were reacted in 20 g of DMF at 90° C. for 14 hr. to give 10.9 g of polymer (yield, 55% of theory). The relative viscosity, ηrel, was 1.10 (0.5 g of polymer per deciliter in dimethylformamide at 25° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05059513 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-54054e46f14e49ae91a415a3df285364 |
| Source note | uspto-grants-1991_10 |