HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 19991746, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 19991788 | HCID 19991788 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19991746 | HCID 19991746 | — |
Reaction Steps
9.7 g of the product from Example 10 are heated under reflux for 3 hours with 50 ml of morpholine. The orange reaction mixture is poured into water. The crude product precipitating during this is dissolved in ethyl acetate and purified chromatographically on an SiO2 column. The purified product is a viscous material.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05059689 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-47e8bebedc6d4f928ef3e9a96362b9b9 |
| Source note | uspto-grants-1991_10 |