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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 346014Generated: October 28, 2026

Phenol → HCID 19600830, compound

https://huagongshe.com/reaction/346014

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenolHCID 996—
ReactantMethyl 3-HydroxybenzoateHCID 88068—
ReactantHCID 86745185HCID 86745185—
ProductHCID 19600830HCID 19600830—

Reaction Steps

By the method of Example 27, substituting the phenol with a molar equivalent of methyl 3-hydroxybenzoate, 7-benzyloxy-4-bromo-3,4-dihydro-1-benzoxepin-(5(2H)-one (17.3 g) was converted to present title product, 10.9 g, m.p. 134°-136° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05059609
Source datasetuspto-grants-1991_10
ORD IDord-20660eca6d224407ab3ab1302d875410
Source noteuspto-grants-1991_10