HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 21868329, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 1-Adamantanecarboxylic acid | HCID 13235 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21868329 | HCID 21868329 | 97% |
Reaction Steps
Stir 1.0 mol of adamantane carboxylic acid in 600 ml of methanol. Under ice cooling, drop 1.53 mol of acetyl chloride into the solution within 1 h. Remove the ice bath, and allow the reaction mixture to reach room temperature. Subsequently, heat for 3 hrs under reflux. Evaporate the reaction mixture to dryness under vacuum and distill. (Yield: 97%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05061703 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-1cc69044c42e4aca89f6ec3faf2da774 |
| Source note | uspto-grants-1991_10 |