HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl mercaptan → 4-(Benzylsulfanyl)benzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl mercaptan | HCID 7509 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | 4-Bromobenzaldehyde | HCID 70741 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(Benzylsulfanyl)benzaldehyde | HCID 12842460 | — |
Reaction Steps
Title product was prepared from benzyl mercaptan (145 mmol, 17.9 g) and 4-bromobenzaldehyde according to the method of Preparation 1 yielding 4 g of purified product following chromatography on silica gel using 9:1 hexane:ethyl acetate as eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05061717 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-86ee962b5fcb4660860a19ce96f5ced4 |
| Source note | uspto-grants-1991_10 |