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HRID346208

反应详情

EQUATION

反应方程式

HRID 346208 的结构方程式

REACTANTS

反应物

3
结构：SCc1ccccc1
HCID7509

Benzenemethanethiol

C7H8S

结构：CCCCCC
HCID8058

n-Hexane

C6H14

结构：O=Cc1ccc(Br)cc1
HCID70741

Benzaldehyde, 4-bromo-

C7H5BrO

PRODUCTS

生成物

1
结构：O=Cc1ccc(SCc2ccccc2)cc1
HCID12842460

4-(Benzylsulfanyl)benzaldehyde

C14H12OS

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Title product was prepared from benzyl mercaptan (145 mmol, 17.9 g) and 4-bromobenzaldehyde according to the method of Preparation 1 yielding 4 g of purified product following chromatography on silica gel using 9:1 hexane:ethyl acetate as eluant.