化工社化工社 化学情報印刷レポート · 研究参考用
4-Bromobenzaldehyde → HCID 19754542、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-Bromobenzaldehyde | HCID 70741 | — |
| 反応物 | 3-Phenylpropane-1-thiol | HCID 90596 | — |
| 生成物 | HCID 19754542 | HCID 19754542 | 101.2% |
反応手順
By the method of Preparation 7, 3-phenylpropyl mercaptan (41.1 g) and 4-bromobenzaldehyde (53.7 g) were converted to 70 g of present title product, isolated as an oil following chromatography on silica gel using 9:1 hexane:ethyl acetate as eluant; tlc Rf 0.4 (1:4 ethyl acetate:hexane).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05061717 |
| 出典データセット | uspto-grants-1991_10 |
| ORD ID | ord-23d754181d1342f6acbf75acdbbf3d71 |
| 出典メモ | uspto-grants-1991_10 |