HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 1,2,2-Trichloro-3,3-dimethylcyclopropanecarboxylic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1,2,2-Trichloro-3,3-dimethylcyclopropanecarboxylic acid | HCID 13654696 | — |
| Product | 1,2,2-Trichloro-3,3-dimethylcyclopropanecarboxylic acid chloride | HCID 13654698 | — |
Reaction Steps
The 1,2,2-trichloro-2,2-dimethylcyclopropanecarboxylic acid (3.0 g) synthesized in Example k and thionyl chloride (1.0 ml) were mixed, and reacted at 60° C. The reaction mixture was distilled under reduced pressure to give the desired 1,2,2-trichloro-3,3-dimethylcyclopropanecarboxylic acid chloride (2.8 g) represented by the following formula. ##STR26##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05061731 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-1c052737bb0341df8b9d2564b4ef283f |
| Source note | uspto-grants-1991_10 |