HRID346539

反应详情

EQUATION

反应方程式

HRID 346539 的结构方程式

PROCEDURE

实验过程

Prepared in analogy to Example 6 with 75 mg (0.17 mmol) of isopropyl-4,6-diamino-2-[1-(2-fluorobenzyl)-1H-pyrazolo[3,4-b]pyridin-3-yl]-5-pyrimidinylcarbamate from Example 3, 10.31 mg (0.26 mmol) of sodium hydride and 24.4 mg (0.17 mmol) of iodomethane. The residue is purified by preparative RP-HPLC.

WORKUP

后处理

  1. customThe residue is purified by preparative RP-HPLC