HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexane → 2-(3-Hydroxyphenyl)-2-oxoacetaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | 3-Hydroxyacetophenone | HCID 8487 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Product | 2-(3-Hydroxyphenyl)-2-oxoacetaldehyde | HCID 12910875 | — |
Reaction Steps
Using 1:1 hexane:ethyl acetate as eluant, the method of Preparation 68 was employed to convert 3-hydroxyacetophenone (15.0 g., 0.11 mol) to present title product, 7.4 g.; 1H-nmr (DMSO-d6) 7.09 (m, 2H), 7.43 (m, 3H), 9.75 (br m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04762921 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-9c67623f0b554c5ea47564486370e681 |
| Source note | uspto-grants-1988_08 |