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HRID34744

反应详情

EQUATION

反应方程式

HRID 34744 的结构方程式

REACTANTS

反应物

3
结构：CCCCCC
HCID8058

n-Hexane

C6H14

结构：CC(=O)c1cccc(O)c1
HCID8487

3-Hydroxyacetophenone

C8H8O2

结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

PRODUCTS

生成物

1
结构：O=CC(=O)c1cccc(O)c1
HCID12910875

未命名化合物

PROCEDURE

实验过程

Using 1:1 hexane:ethyl acetate as eluant, the method of Preparation 68 was employed to convert 3-hydroxyacetophenone (15.0 g., 0.11 mol) to present title product, 7.4 g.; 1H-nmr (DMSO-d6) 7.09 (m, 2H), 7.43 (m, 3H), 9.75 (br m, 1H).